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standard pulse sequences from the bruker library  (Bruker Corporation)

 
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    Bruker Corporation standard pulse sequences from the bruker library
    Standard Pulse Sequences From The Bruker Library, supplied by Bruker Corporation, used in various techniques. Bioz Stars score: 90/100, based on 1 PubMed citations. ZERO BIAS - scores, article reviews, protocol conditions and more
    https://www.bioz.com/product/standard+pulse+sequence+from+the+bruker+library/bruker+pulse+sequences/pmc12044470-44-22-22
    Average 90 stars, based on 1 article reviews
    standard pulse sequences from the bruker library - by Bioz Stars, 2026-10
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    Sequencing:

    Article Title: Molecular basis for the preferential recognition of β1,3-1,4-glucans by the family 11 carbohydrate-binding module from Clostridium thermocellum.
    Article Snippet: The experimental conditions for the data acquisition were as follows: 1H NMR – a standard pulse sequence from the Bruker library was used [38] with a 90o flip angle of 8.05 μs at 3.50 dB, acquisition time 5.46 s, spectral window of 3000 Hz centred at 2824.8 Hz, 32 transients with 32 K data points, relaxation delay of 1.0 second and digital resolution of 0.09 Hz per point. .. Water suppression was accomplished using excitation sculpting with gradients [38] using a 180o shaped pulse (Sinc1.1000) with 2000 ms at 40.78 dB; 1H-1H-COSY – a standard pulse sequence from the Bruker library was used (cosygpppprqf) with 4 transients acquired in a matrix with 4096 data points in t2 in a spectral window of 3000 Hz, centered at 2824.8 Hz and 512 increments in t1 with a relaxation delay of 1 s and an acquisition time of 0.68 s; 1H-13C-HSQC – a standard pulse sequence from the Bruker library was used [39–41] with 4 transients in a matrix with 1024 data points in t2 in a spectral window of 3000 Hz centred at 2824.8 Hz and with 256 increments in t1 in a spectral window of 21128 Hz centred at 11314.0 Hz and with a relaxation delay of 1.5 s and an acquisition time of 0.17 s. A delay of 1.72 ms was used for the evolution of the 1 bond CH coupling calculated for 1J(C,H) = 145 Hz; 1H-13C-HSQC-TOCSY – a standard pulse sequence from the Bruker library was used (hsqcdiedetgpsisp.1) with 8 transients in a matrix with 1024 data points in t2 in a spectral window of 3000 Hz centred at 2824.8 Hz and with 256 increments in t1 in a spectral window of 25000 Hz centred at 11314.0 Hz and with a relaxation delay of 1.5 s and an acquisition time of 0.17 s. A delay of 1.72 ms was used for the evolution of the 1 bond CH coupling calculated for 1J(C,H) = 145 Hz. .. Water suppression was accomplished using excitation sculpting with gradients [38] using a 180o shaped pulse (Sinc1.1000) with 2000 ms at 40.78 dB; 1H-1H-COSY – a standard pulse sequence from the Bruker library was used (cosygpppprqf) with 4 transients acquired in a matrix with 4096 data points in t2 in a spectral window of 3000 Hz, centered at 2824.8 Hz and 512 increments in t1 with a relaxation delay of 1 s and an acquisition time of 0.68 s; 1H-13C-HSQC – a standard pulse sequence from the Bruker library was used [39–41] with 4 transients in a matrix with 1024 data points in t2 in a spectral window of 3000 Hz centred at 2824.8 Hz and with 256 increments in t1 in a spectral window of 21128 Hz centred at 11314.0 Hz and with a relaxation delay of 1.5 s and an acquisition time of 0.17 s. A delay of 1.72 ms was used for the evolution of the 1 bond CH coupling calculated for 1J(C,H) = 145 Hz; 1H-13C-HSQC-TOCSY – a standard pulse sequence from the Bruker library was used (hsqcdiedetgpsisp.1) with 8 transients in a matrix with 1024 data points in t2 in a spectral window of 3000 Hz centred at 2824.8 Hz and with 256 increments in t1 in a spectral window of 25000 Hz centred at 11314.0 Hz and with a relaxation delay of 1.5 s and an acquisition time of 0.17 s. A delay of 1.72 ms was used for the evolution of the 1 bond CH coupling calculated for 1J(C,H) = 145 Hz.



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